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Research Laboratory

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Field Emission Scanning Electron Microscope (FESEM)

Materials Characterization

Starting from৳11,456
All services

FESEM provides ultra-high-resolution imaging for studying surface morphology, microstructure, particle size, grain boundaries, fractures, coatings, and defects. With an EDS detector, qualitative and semi-quantitative elemental composition can also be determined.

Test specification

Methodology
  • Field Emission Scanning Electron Microscopy (FESEM)
  • Secondary Electron Imaging (SE)
  • Backscattered Electron Imaging (BSE)
Standards followed
  • ASTM E766
  • ASTM E986
  • ASTM E1508
  • ISO 16700
  • ISO 22309 (where applicable)
Equipment used
  • FESEM
  • Secondary Electron Detector
  • Backscattered Electron Detector
  • Motorized Specimen Stage
  • High Vacuum System
Parameters measured
  • Surface morphology
  • particle shape/size
  • grain size/distribution
  • surface defects
  • surface roughness (qualitative)
  • crack formation
  • fracture features
  • porosity
  • coating thickness (cross-sectional)
  • fiber diameter
  • layer structure
Measurement range
  • Magnification 20x-1,000,000x
  • Accelerating Voltage 0.5-30 kV
  • Working Distance 1-40 mm
  • Resolution <=1.5 nm
Accuracy / detection limit
  • Imaging Resolution: <=1.5 nm
  • Image Magnification Accuracy: as per manufacturer specification

Suitability

Applications
Materials ScienceMetallurgical EngineeringMechanical EngineeringNanotechnologySemiconductor ResearchBattery MaterialsComposite MaterialsPolymer EngineeringBiomedical MaterialsThin Film TechnologyCorrosion EngineeringFailure InvestigationAdditive ManufacturingGeological Materials
Industries served
UniversitiesResearch InstitutesSteel IndustryCement IndustryCeramic IndustryElectronics IndustryPharmaceutical IndustryEnergy SectorAerospaceAutomotiveTextile Industry
Advantages
  • Ultra-high spatial resolution
  • non-destructive characterization
  • excellent depth of field
  • rapid analysis
  • suitable for micro- and nanomaterials
Limitations
  • Non-conductive samples require conductive coating
  • samples must fit within the specimen chamber
  • FESEM does not directly identify crystal phases (XRD recommended for phase analysis)

Submitting a sample

Sample requirement
  • Sample should be clean and dry
  • loose contamination removed
  • non-conductive samples require Au/Pt/Carbon coating
  • maximum dimensions depend on specimen chamber capacity
  • cross-sectional samples should be properly polished when required
Turnaround time
  • Standard Service: 3-5 Working Days
  • Urgent Service: 24-48 Hours (subject to availability)
Deliverables
  • High-resolution FESEM images
  • PDF test report
  • TIFF images
  • JPEG images
  • observation summary
  • interpretation (optional)

Request this test

Send us your sample details and we'll confirm scope and timing.

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